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Diethyl succinate synthesis by reactive distillation

✍ Scribed by Alvaro Orjuela; Aspi Kolah; Xi Hong; Carl T. Lira; Dennis J. Miller

Book ID
113901266
Publisher
Elsevier Science
Year
2012
Tongue
English
Weight
977 KB
Volume
88
Category
Article
ISSN
1383-5866

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Diethyl phosphonomethyltriflate, prepared from diethyl hydroxymethylphosphonate, readily reacts in good to excellent yields with a variety of oxygen and nitrogen nucleophiles. Currently, no mild method exists for effecting displacement reactions on the a-carbon of phosphonates. Such a reaction woul