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Diethyl 4-(4-tert-butylphenyl)pyridine-2,6-dicarboxylate

✍ Scribed by Santoni, Marie-Pierre C. ;Fang, Yuan-Qing ;Hanan, Garry S. ;Proust, Anna ;Hasenknopf, Bernold

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
344 KB
Volume
63
Category
Article
ISSN
1600-5368

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pounds, presumably oligomers. In glacial acetic acid (CH3C0,H/CH2C12=3 :2, i=40 mA/cm2, T=2OoC, Pt electrode) 17% androstanyl acetate is obtained and 38% androstane is recovered. Remarkable is the selectivity of the oxidation: We found that the 6-(6a), 7-, and 12-acetates are formed in the ratio 35