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Die Strukturen der mittleren Ringverbindungen VI. 1,6-trans-Diaminocyclodecan-dihydrochlorid

✍ Scribed by Effi Huber-Buser; J. D. Dunitz


Publisher
John Wiley and Sons
Year
1961
Tongue
German
Weight
414 KB
Volume
44
Category
Article
ISSN
0018-019X

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✦ Synopsis


The structure determination of the triclinic crystal modification of 1,6‐trans‐ diaminocyclodecane dihydrochloride has been refined by three‐dimensional least squares analysis of about 1300 reflexions. The earlier results derived by two‐dimensional methods are confirmed, but with a considerable improvement in the accuracy.


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The structure determination of the triclinic crystal modification of 1,6-transdiaminocyclodecane dihydrochloride has been refined by three-dimensional least squares analysis of about 1300 reflexions. The earlier results derived by two-dimensional methods are confirmed, but with a considerable improv

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## Abstract 1,6‐__trans__‐diaminocyclodecane dihydrochloride crystallizes in triclinic and monoclinic modifications. The structure of the triclinic form with __a__ = 9,02; __b__ = 6,19; __c__ = 6,20 Γ…; Ξ± = 96,7Β°; Ξ² = 99,3Β°; Ξ³ = 108,1Β°; space group P1; __Z__ = 1, has been determined by analysis of t

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