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Diazabicycloalkanes with bridgehead nitrogen atoms. 19. Reactions of monoquaternary salts of dibenzo[b,e]-1,4-diazabicyclo[2.2.2]octadiene with nucleophilic reagents

โœ Scribed by N. P. Lukyanchuk; V. N. Sil'nikov; G. V. Shishkin


Publisher
Springer US
Year
1989
Tongue
English
Weight
241 KB
Volume
25
Category
Article
ISSN
0009-3122

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Diazabicycloalkanes with nitrogen atoms
โœ N. P. Luk'yanchuk; N. I. Sagalaeva; V. K. Soboleva; G. V. Shishkin ๐Ÿ“‚ Article ๐Ÿ“… 1987 ๐Ÿ› Springer US ๐ŸŒ English โš– 588 KB

3, 5, isoquinoline (Ilia). A mixture of 2.27 g (i0 mmole) of compound IIa and 0.68 ml (15 mmole) of hydrazine hydrate was boiled in ethanol for 3 h. On cooling, hydrazone IIIa formed a precipitate, which was filtered off, dried, and recrystallized. ## 2-Semicarbazono-3-oxo-5,5-dimethyl-2,3~5,6-te