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Diastereoselective synthesis and bioactivity of long-chain anti-2-amino-3-alkanols

✍ Scribed by Bi-Shuang Chen; Long-He Yang; Jian-Liang Ye; Tao Huang; Yuan-Ping Ruan; Jin Fu; Pei-Qiang Huang

Book ID
113583131
Publisher
Elsevier Science
Year
2011
Tongue
French
Weight
585 KB
Volume
46
Category
Article
ISSN
0223-5234

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## Abstract Benzaldehyde adds to 1‐pyrrolidinylcyclohexene under mild conditions giving the amino ketone 3a. The unstable ketone was reduced to the epimeric alcohols 4 and 5, the stereochemistry of which was determined by 2D‐NMR correlation spectroscopy.