Di-μ-methoxo-bis{[2,3-dimethylbutane-2,3-diolato(1–)]-cis-dioxomolybdenum (VI)}–methanol (1/2)
✍ Scribed by Knobler, C. B. ;Penfold, B. R. ;Robinson, W. T. ;Wilkins, C. J.
- Book ID
- 114527705
- Publisher
- International Union of Crystallography
- Year
- 1981
- Weight
- 295 KB
- Volume
- 37
- Category
- Article
- ISSN
- 0567-7408
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 150 K Mean '(C±C) = 0.010 A Ê R factor = 0.023 wR factor = 0.053 Data-to-parameter ratio = 12.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, [Cr 2 (CH 3 O) 2 (C 15 H 11 O 2 ) 4 ], was obtained from the reaction of [CrCl 3 (C 4 H 8 O) 3 ] with 1,3-diphenylpropane-1,3-dione and sodium methoxide in anydrous methanol. Its structure consists of discrete molecules, in which two centrosymmetrically related chromium(III) ions