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Development of a Novel Ionic Support and Its Application in the Ionic Liquid Phase Assisted Synthesis of a Potent Antithrombotic.

✍ Scribed by Martin de Kort; Adriaan W. Tuin; Suzanne Kuiper; Hermen S. Overkleeft; Gijs A. van der Marel; Rogier C. Buijsman


Publisher
John Wiley and Sons
Year
2004
Weight
157 KB
Volume
35
Category
Article
ISSN
0931-7597

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Synthesis of the novel ionic liquid [N-p
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## Abstract The novel, low‐melting‐point (19 Β°C) salt [__N__‐pentylpyridinium]^+^ [__closo__‐CB~11~H~12~]^βˆ’^ (2) was synthesized in 93% yield and characterized by elemental analysis, IR spectroscopy, and ^1^H, ^13^C, and ^11^B NMR spectroscopy. The salt was used as a solvent in several dehalogenati