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Determination of Wear Metals in Marine Lubricating Oils by Microwave Digestion and Atomic Absorption Spectrometry

✍ Scribed by Sanz-Segundo, Celestino ;Hernández-Artiga, María P. ;Hidalgo-Hidalgo de Cisneros, José L. ;Bellido-Milla, Dolores ;Naranjo-Rodriguez, Ignacio

Publisher
Springer-Verlag
Year
1999
Weight
71 KB
Volume
132
Category
Article
ISSN
0344-838X

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The use of several acid mixtures for digestion of marine biological materials with microwaveassisted heating was investigated. The mixtures of HNO 3 -H 2 SO 4 -H 2 O 2 and of HNO 3 -H 2 SO 4 -HCl were most effective after microwave digestion, resulting in complete decomposition of samples. Recoverie