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Determination of the crystal structure and the absolute configuration of (+)-2,2'-dihydroxy-1,1'-binaphthalene-3,3'-dicarboxylic acid dimethyl ester bromobenzene solvate

✍ Scribed by Akimoto, H. ;Iitaka, Y.


Book ID
117856696
Publisher
International Union of Crystallography
Year
1969
Weight
1022 KB
Volume
25
Category
Article
ISSN
0567-7408

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NMR determination of the absolute config
✍ Hiroki Fukui; Yukiharu Fukushi; Satoshi Tahara πŸ“‚ Article πŸ“… 2003 πŸ› Elsevier Science 🌐 French βš– 218 KB

Each of the chiral 1,2-and 1,3-diols examined was derivatized exclusively to a single diastereomeric acetal by the use of a new axially chiral reagent, 2%-methoxy-1,1%-binaphthalene-8-carbaldehyde (MBC). The absolute configuration of the original 1,2-and 1,3-diols was determined by the NOE correlati