✦ LIBER ✦

Determination of sulfonamides in livers using matrix solid-phase dispersion extraction high-performance liquid chromatography

✍ Scribed by Yupu Zhang; Xu Xu; Xiao Qi; Wenquan Gao; Shuo Sun; Xiaotian Li; Chengfei Jiang; Aimin Yu; Hanqi Zhang; Yong Yu

Publisher: John Wiley and Sons
Year: 2011
Tongue: English
Weight: 310 KB
Volume: 35
Category: Article
ISSN: 1615-9306
DOI: 10.1002/jssc.201100600

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

The matrix solid‐phase dispersion (MSPD) was applied for extracting seven sulfonamides (SAs) in liver samples. The separation and determination were carried out by high‐performance liquid chromatography. The analytes were derivated with fluorescamine and detected with fluorescence detector. The types of dispersion adsorbents for MSPD were examined and the highest recovery was obtained when the diatomaceous earth was used as the dispersion adsorbent and the mass ratio of dispersion adsorbent to sample was 3:1. The acetone was used as the elution solvent. Under the optimal conditions, the linear range for determining the SAs in liver samples was 5.0–1000.0 ng/g. The porcine, chicken and cattle liver samples were analyzed and the average recoveries of seven SAs were higher than 84.6%.

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