𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Determination of Polycyclic Aromatic Hydrocarbons in Oyster Tissues by High-Performance Liquid Chromatography with Ultraviolet and Fluorescence Detection

✍ Scribed by D. Thompson; D. Jolley; W. Maher

Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
478 KB
Volume
47
Category
Article
ISSN
0026-265X

No coin nor oath required. For personal study only.

✦ Synopsis

Polycyclic aromatic hydrocarbons ( (\mathrm{PAHs}) ) in oyster tissues were isolated by saponification with aqueous potassium hydroxide and hexane partitioning. Extracts were purified by adsorption chromatography using silicic acid and alumina oxide followed by gel chromatography with either Sephadex LH-20 or Bio-Beads S.X8. Measurement of PAHs were performed by high-performance liquid chromatography (HPLC) with ultraviolet absorbance and fluorescence detection. Recovery trials using NBS 1647a-spiked oyster homongenates revealed that the use of adsorption chromatography followed by gel chromatography was not effective in purifying extracts to allow the determination of lower ring PAH by HPLC or higher ring PAH by gas chromatography-mass spectrometry. O 1993 Academic Press, Inc.

πŸ“œ SIMILAR VOLUMES

High-performance liquid chromatography d
High-performance liquid chromatography determination of nitrated polycyclic aromatic hydrocarbons by indirect fluorescence detection
✍ Salma M. Al-Kindy; James N. Miller πŸ“‚ Article πŸ“… 2009 πŸ› John Wiley and Sons 🌐 English βš– 112 KB πŸ‘ 2 views

## Abstract A high‐performance liquid chromatography (HPLC) method for the analysis of nitrated polcyclic aromatic hydrocarbons (NPAHs) is reported. NPAH mixtures were pre‐concentrated using solid‐phase extraction and well resolved on a C~18~ column. They were detected using an indirect method invo

Determination of Diethylstilbestrol in A
Determination of Diethylstilbestrol in Aquatic Products by High Performance Liquid Chromatography with Fluorescence Detection
✍ Yingjiang Xu; Jinpei Geng; Xiuzhen Zhang; Shijuan Zhang; Xiuhui Tian; Huihui Liu πŸ“‚ Article πŸ“… 2010 πŸ› John Wiley and Sons 🌐 English βš– 65 KB

## Abstract A sensitive method for the determination of diethylstilbestrol (DES) in aquatic products by high performance liquid chromatography (HPLC) using a fluorescence detector (FLD) was developed. By means of sulfonation in concentrated sulfuric acid and hydrolysis, DES was converted into a rea

Determination of atrasentan by high perf
Determination of atrasentan by high performance liquid chromatography with fluorescence detection in human plasma
✍ Peter D. Bryan; Lisa B. Sapochak; Michelle M. Tames; Robert J. Padley; Tawakol A πŸ“‚ Article πŸ“… 2001 πŸ› John Wiley and Sons 🌐 English βš– 108 KB πŸ‘ 2 views

Atrasentan is an endothelin antagonist selective for the ET A receptor in development at Abbott Laboratories for the treatment of cardiovascular disease and cell proliferation disorders. A simple and sensitive chromatographic method for the determination of atrasentan in human plasma has been develo