Determination of phenolic compounds in olives by reversed-phase chromatography and mass spectrometry
β Scribed by Danielle Ryan; Kevin Robards; Shimon Lavee
- Book ID
- 108341626
- Publisher
- Elsevier Science
- Year
- 1999
- Tongue
- English
- Weight
- 164 KB
- Volume
- 832
- Category
- Article
- ISSN
- 1873-3778
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An analytical procedure for the determination of phenyltin compounds in environmental sample waters was studied. Chromatography of mono-, di-tri-phenyltin (MPT, DPT and TPT) was performed on a reversed-phase C 18 column with the mobile phase comprising methanol/10 Οͺ 2 M H 3 PO 4 (80 : 20 v/v) at pH
Phenol and monochlorophenols were determined by reversed-phase liquid chromatography with LiChrospher RP-18e. A good separation was obtained with this system. The effectiveness of liquid-liquid and solid-phase extractions on Amberlite XAD-2, XAD-4, octadecyl Si 100, Tenax and Polyspher RP-18 were co