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Determination of light elements using x-ray spectrometry. Part I—Analytical implications of using scattered tube lines

✍ Scribed by Hans A. van Sprang; Mirjan H. J. Bekkers

Publisher: John Wiley and Sons
Year: 1998
Tongue: English
Weight: 310 KB
Volume: 27
Category: Article
ISSN: 0049-8246
DOI: 10.1002/(sici)1097-4539(199801/02)27:1<31::aid-xrs245>3.0.co;2-#

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✦ Synopsis

X-rays scattered from a material contain information on the composition of the sample. The relationship between the sample composition and the amount of scattered radiation was studied for low-Z materials. Use of Comptonscattered tubelines appears to be the preferred technique and a calibration is presented based on a set of standards of known composition. Some unexpected features are discussed and the possible use of this method for quantiÐcation is demonstrated using results from a second set of standards. 1998

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Two methods that allow the determination of the boron content in a glass or a Ñux were compared. The Ðrst method uses direct measurement of B Ka Ñuorescence and subsequent fundamental parameter-based quantiÐcation. Although it can be used for low concentrations of B, it requires extra care with cali