A method is described for simultaneous determination of 14 lanthanides and yttrium in monazites and xenotimes by inductively-coupled plasma atomic emission spectrometry. The ore samples were decomposed by heating with nitric acid/perchloric acid or hydrofluoric/nitric/perchloric acids, or sulfuric a
Determination of lanthanides and yttrium in rare earth ores and concentrates by inductively coupled plasma atomic emission spectrometry
β Scribed by M.I. Rucandio
- Publisher
- Elsevier Science
- Year
- 1992
- Tongue
- English
- Weight
- 940 KB
- Volume
- 264
- Category
- Article
- ISSN
- 0003-2670
No coin nor oath required. For personal study only.
β¦ Synopsis
An mductlvely coupled plasma atomic emlsslon spectrometrlc WP-AES) method for the determmatlon of lanthamdes and yttrmm m rare earth ores and concentrates 1s described After a smtable separation of these elements from the other matru( constituents, a mtnc solution of rare earth elements was obtained for the ICP-AES measurements
The optunum condltlons were selected by a simplex method Several analytlcal wavelengths were chosen for each element, using barmm as mtemal standard A detaded study of spectral interferences was made and correctlon coefficients were calculated Good agreement between the results and previously published values obtamed by several techmques was obtamed
π SIMILAR VOLUMES
The chromatographlc separation of rare earth elements (REEs), prior to mductlvely coupled plasma atomic emlsslon spectrometrlc (ICP-AES) measurements, usmg a column packed Hrlth 2-ethylhexyl hydrogen 2-ethylhexylphosphonate (PC-88A)\_loaded polymer resm m order to exclude spectral Interferences was
An existing method for cold vapour generation and inductively coupled plasma atomic emission spectroscopy (ICPAES) has been extended to enable the determination of mercury concentrations in solutions by inductively coupled plasma mass spectrometry (ICPMS). mpical instrument variability (3u of blank)
A simple and rapid method has been developed for the determination of molybdenum and vanadium in seawater using ion-exchange preconcentration and inductively coupled plasma atomic emission spectrometry (ICP-AES). One hundred milliliters of seawater prepared as \(0.05 M\) hydrochloric acid solution i
Continuous flow generation of two different types of volatile lead species, PbH, (NaBH, as the reducing agent) or tetraethyllead (NaBEt, as the alkylating agent) as a means of gaseous sample introduction for inductively coupled plasma atomic emission spectrometry (ICP-f&S) have been investigated in