𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Determination of Internuclear Distances in Uniformly Labeled Molecules by Rotational-Resonance Solid-State NMR

✍ Scribed by Williamson, Philip T. F.; Verhoeven, Aswin; Ernst, Matthias; Meier, Beat H.


Book ID
127161172
Publisher
American Chemical Society
Year
2003
Tongue
English
Weight
152 KB
Volume
125
Category
Article
ISSN
0002-7863

No coin nor oath required. For personal study only.


πŸ“œ SIMILAR VOLUMES


13C/15N distance determination by CPMAS
✍ Maggy Hologne; JΓ©sus Raya; JΓ©rΓ΄me Hirschinger πŸ“‚ Article πŸ“… 2006 πŸ› John Wiley and Sons 🌐 English βš– 216 KB

The REDOR and CPMAS techniques are applied for measuring 13C-15N dipolar coupling constants in glycine. It is shown that the selective CP or SPECIFIC CP technique removes the coherent evolution of the spin system under homonuclear 13C-13C J couplings. While the large coupling constant (approximately

Conformational constraints in solid-stat
✍ Nathan A. Oyler; Robert Tycko πŸ“‚ Article πŸ“… 2007 πŸ› John Wiley and Sons 🌐 English βš– 458 KB

A solid-state nuclear magnetic resonance (NMR) technique is described for obtaining constraints on the backbone conformation of a protein or peptide that is prepared with uniform 15 N, 13 C labeling of consecutive pairs of amino acids or of longer segments. The technique, called double single-quantu

Measurement of Internuclear Distances in
✍ Frederick G Vogt; Susan M Mattingly; James M Gibson; Karl T Mueller πŸ“‚ Article πŸ“… 2000 πŸ› Elsevier Science 🌐 English βš– 106 KB

A background-filtered version of the rotational-echo double resonance (REDOR) experiment is demonstrated. The experiment combines a traditional REDOR pulse sequence with a double-cross-polarization (DCP) sequence to select only those signals coming from spin pairs of interest. The relatively ineffic