Determination of hexachlorocyclohexanes in ground water by coupled liquid-liquid extraction and capillary gas chromatography
โ Scribed by Goosenes, E. C. ;Bunschoten, R. G. ;Engelen, V. ;de Jong, D. ;van den Berg, J. H. M.
- Publisher
- John Wiley and Sons
- Year
- 1990
- Tongue
- English
- Weight
- 455 KB
- Volume
- 13
- Category
- Article
- ISSN
- 0935-6304
No coin nor oath required. For personal study only.
โฆ Synopsis
Journal of High Resolution Chromatography layer was evaporated till 1 ml and cleaned up over a deactivated aluminum oxide column. After elution with hexane, 1 p1 of the organic Phase was injected (split ratio 1 : 20) onto a 50 m 0.32 mm i.d. CP-Si1 19CB column (df = 0.12 ym)l).
๐ SIMILAR VOLUMES
## Abstract A critical study of a solid phase extraction method using C~18~ SPE columns for the determination of 23 halogenated pesticides is presented. Type of sorbent, sorbent mass, flow rate in the extraction process, sample concentration of the different compounds, sample volume, pH, ionic stre
## Abstract A simple and rapid method based on homogeneous liquidโliquid extraction coupled to HPLC with fluorescence detection was developed for the determination of aflatoxin B1 (AFB1) in the rice and grain samples after postโcolumn derivatization. The proposed method eliminated the use of immuno
A method for routine small-volume solvent extraction, derivitization and gasliquid chromatographic analysis of methylmalonic and succinic acids is described. The procedure allows for quantitative determination of mass and radioactivity of these acids and can be applied to metabolic studies of the ge