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Determination of Aldehydes in Presence of Ketones: And Procedure for Acetals

โœ Scribed by Siegel, H.; Weiss, F. T.


Book ID
126903575
Publisher
American Chemical Society
Year
1954
Tongue
English
Weight
378 KB
Volume
26
Category
Article
ISSN
0003-2700

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A convenient one-pot procedure for the s
โœ Mario Paglialunga Paradisi; Giampiero Pagani Zecchini; Giorgio Ortar ๐Ÿ“‚ Article ๐Ÿ“… 1980 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 212 KB

The title process has been accomplished by a three-step sequence involving protection of aldeh;de as the imine, in situ reduction of ketone with lithium tri-tert-butoxyaluminohydride, and regeneration of aldehyde on hydrolytic work-up. The preferential in situ ketalization or hydration of aldehydes