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Determination of acephate, methamidophos and monocrotophos in crude palm oil

✍ Scribed by Chee Beng Yeoh; Ainie Kuntom; Selvarajan Dorasamy; Mohd Rizal Omar; Muhd Yusof Mohd Nor; Mohd Razali Mohd Noh


Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
272 KB
Volume
108
Category
Article
ISSN
1438-7697

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✦ Synopsis


Determination of acephate, methamidophos and monocrotophos in crude palm oil

A method for the determination of acephate, methamidophos and monocrotophos in oil matrices is described. Pesticide residues in crude palm oil were extracted with acetonitrile, and a clean-up process was performed by cooling the entire extract below 10 7C, followed by a discolouring process using a Carbograph SPE cartridge. The extract was analysed using gas chromatography coupled with a pulsed flame photometry detector. The limit of detection for the method was calculated from regression data, and the recovery test results were in the range of 85-109%.


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