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Detection of environmental polyorganosiloxanes (silicones) by silicon-29 NMR spectroscopy

✍ Scribed by Jon M Bellama; Stephen R Meyer; Robert E Pellenbarg


Publisher
John Wiley and Sons
Year
1991
Tongue
English
Weight
257 KB
Volume
5
Category
Article
ISSN
0268-2605

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The synthesis and characterization of 1,3,10,12-tetraoxo-2,11-(diphenylsilylene)[5.5]paracyclophane obtained by reaction of 1,4-benzenedimethanol and dichlorodiphenylsilane is reported. The structure was established by mass spectrometry; 1 H, 13 C, and 29 Si NMR; and X-ray diffraction analysis.