𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Derivatization with fluorogenic benzofurazan reagents of amino acid enantiomers and their separation on a pirkle column

✍ Scribed by Kazuhiro Imai; Takeshi Fukushima

Publisher
John Wiley and Sons
Year
1993
Tongue
English
Weight
214 KB
Volume
7
Category
Article
ISSN
0269-3879

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Sensitive determination of enantiomers o
Sensitive determination of enantiomers of amino acids derivatized with the fluorogenic reagent, 4-fluoro-7-nitro-2,1,3-benzoxadiazole, separated on a pirkle-type column, sumichiral OA 2500(S)
✍ Kazuhiro Imai; Takeshi Fukushima; Sonoko Uzu 📂 Article 📅 1993 🏛 John Wiley and Sons 🌐 English ⚖ 159 KB 👁 2 views

Some L-and D-amino acids (Phe or Leu) were derivatized with a fluorogenic reagent, 4-fluoro-7-nitro-2,1,3benzoxadiazole (NBD-F) and separated on a Pirkle-type column, Sumichiral OA 2500(S) [(S)-1-naphthylglyeyl-3,5-dinitrophenylamide silica gel] with a mobile phase of 20mM ammonium acetate in methan

GC separation of amino acid enantiomers
GC separation of amino acid enantiomers via derivatization with heptafluorobutyl chloroformate and Chirasil-L-Val column
✍ Helena Zahradníčková; Petr Hušek; Petr Šimek 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 158 KB

## Abstract Heptafluorobutyl chloroformate (HFBCF), a recently introduced derivatization reagent, was examined in enantioseparation of amino acids (AAs) by GC. Twenty proteinogenic AAs, plus ornithine, cystine and 4‐fluorophenylalanine (internal standard) were treated with the reagent and separatio

Separation of N-0437 enantiomers by RP-H
Separation of N-0437 enantiomers by RP-HPLC after pre-column derivatization with D(+)-glucuronic acid
✍ Gerding, T. K. ;Drenth, B. F. H. ;de Zeeuw, R. A. 📂 Article 📅 1987 🏛 John Wiley and Sons 🌐 English ⚖ 238 KB

adducts are destroyed coelutes with the isooctane. Peaks of ## Short Communications Table 1 retention time 2.63,5.44, and 7.65 minutes are from the reagent. Even though these peaksarequitelarge,theydo not interferewith the analysis of the esters. ## Retention data for tert-butyldimethylsilyl est

The factors that influence the elution o
The factors that influence the elution order for the resolution of amino acids on vancomycin phase using the polar-organic mobile phases after their pre-column derivatization with electrophilic reagents
✍ S. Chen 📂 Article 📅 2005 🏛 John Wiley and Sons 🌐 English ⚖ 370 KB 👁 1 views

## Abstract A variety of amino acids were enantioresolved on a vancomycin bonded chiral phase using the polar‐organic mobile phases after their pre‐column derivatization with electrophilic reagents in alkaline medium. The resolution was highly dependent on the analyte's structure and was enhanced a

Separation of free amino acids and catec
Separation of free amino acids and catecholamines in human plasma and rabbit vitreous samples using a new fluorogenic reagent 3-(4-bromobenzoyl)-2-quinolinecarboxaldehyde with CE-LIF detection
✍ Niu Zhang; Hua-Shan Zhang; Hong Wang 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 289 KB 👁 1 views

## Abstract A sensitive and efficient analysis of amino acids and catecholamines is currently presented with 3‐(4‐bromobenzoyl)‐2‐quinolinecarboxaldehyde as a fluorogenic derivatization reagent using CE separation with LIF detection. For good derivatization conditions, the reagent concentrations, p