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Deprotection of N-Tosylated Indoles and Related Structures Using Cesium Carbonate.

✍ Scribed by Joginder S. Bajwa; Guang-Pei Chen; Kapa Prasad; Oljan Repic; Thomas J. Blacklock

Book ID
101996245
Publisher
John Wiley and Sons
Year
2006
Weight
21 KB
Volume
37
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

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A mild, efficient and selective deprotec
A mild, efficient and selective deprotection of t-butyldimethylsilyl-protected phenols using cesium carbonate
✍ Zhi-Yong Jiang; Yan-Guang Wang πŸ“‚ Article πŸ“… 2003 πŸ› Elsevier Science 🌐 French βš– 143 KB

A mild and efficient method for the deprotection of aryl t-butyldimethysilyl (TBS) ethers is described. The protecting group TBS could be cleaved from aryl silyl ethers using cesium carbonate in DMF-H 2 O at room temperature to give the corresponding phenols in excellent yields. The reaction conditi