Early work on preparing carbon-carbon composites by using chemical vapor infiltration is discussed. Later work showed little influence of substrate on infiltration kinetics. and confirmed earlier relationships between property values and density. Yields of total carbon, soot, and CVD carbon are expl
Densification of carbon/carbon composites by pulse chemical vapor infiltration
β Scribed by Hyeok Je Jeong; Hee Dong Park; Jae Do Lee; Jong Ook Park
- Publisher
- Elsevier Science
- Year
- 1996
- Tongue
- English
- Weight
- 508 KB
- Volume
- 34
- Category
- Article
- ISSN
- 0008-6223
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β¦ Synopsis
Two-dimensional carbon/carbon composites were densified with carbon by pyrolysis of propane using the pulse chemical vapor infiltration (CVI) process which repeats the cycle of evacuation and introduction of gas. The experimental parameters were deposition temperature, reactant gas concentration, flow rate, gas introduction time, evacuation time, and pulse number. The most effective parameters of pulse CVI to densify carbon/carbon composites are deposition temperature and gas introduction time. There was a deposition temperature at which the deposition rate was maximum. At higher deposition temperatures, soot was formed. When the gas introduction time was long, bulk density was higher and infiltration uniformity was better. Through these experiments, the optimum experimental condition for densification was found.
π SIMILAR VOLUMES
An analysis of the reaction and diffusion of gases occurring simuitaneously with deposition of carbon in a porous material is presented. The model incorporates a scheme for the formation of carbon during the pyrolysis of a gaseous hydrocarbon to yield predictions for concentration and porosity profi
## Abstrad-Tensile tests have been performed on carbon/carbon composites made from carbon cloths and a pyrolytic carbon matrix and their failure surfaces were examined by scanning electron microscopy. The load-extension curves are characterized by three distinct regions: the applied load needed to
AASTRACTS 331 ment. The electron microscope (both in the scanning and transmission modes) was used to examine the topography of both wet (60% HNOs, 118Β°C) and dry oxidized (air, 700Β°C) fibers as well as fracture surfaces of composites made with treated and untreated fibers. The flexural strength of
A 23 factorial statistically designed experiment was used to study fabrication of carbon/carbon composites using the forced flow-thermal gradient chemical vapor infiltration process. Propane, diluted with hydrogen, was used as the feed. The independent variables were the temperature of the bottom of
Carbon/carbon composites with porosities as low as 7% were fabricated within 8-12 hours using the forced flow-thermal gradient chemical vapor infiltration (FCVI) process. Preforms consisting of 40 layers of T-300 plain weave carbon cloth were infiltrated with a feed containing a carbon source and a