cyclo-Bis[2-methylsulfanyl-6-([1,3,4]thiadiazol-2-ylsulfanylmethyl)pyridinium] diperchlorate
✍ Scribed by Chan, Kannie Wai Yan ;Yang, Chi ;Szeto, Lap
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 207 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 301 K Mean '(C±C) = 0.005 A Ê R factor = 0.080 wR factor = 0.051 Data-to-parameter ratio = 13.1
For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê Disorder in main residue R factor = 0.059 wR factor = 0.114 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 19 H 18 N 2 O 4 S, was synthesized by the reaction of methyl (2-hydroxyphenyl)acetate and 3-(4-methylthio)phenyl-5-chloromethyl-1,2,4-oxadiazole. The structure exhibits intermolecular CÐHÁ Á ÁO hydrogen bonds and CÐ HÁ Á Á% interactions.
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.006 A Ê Disorder in main residue R factor = 0.052 wR factor = 0.156 Data-to-parameter ratio = 16.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 16 H 13 BrOS, was prepared by the Lewis acid-catalysed reaction of 4 0 -bromo-1,1 0 -biphenyl-4-ol withchloro--(methylsulfanyl)acetone. The crystal structure is stabilized by a C-HÁ Á Á interaction involving a CH group of the 4-bromophenyl ring and the furan ring.