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Cyclization in the Course of Clarke—Eschweiler Methylation 1

✍ Scribed by Cope, Arthur C.; Burrows, W. Dickinson

Book ID
118209533
Publisher
American Chemical Society
Year
1965
Tongue
English
Weight
381 KB
Volume
30
Category
Article
ISSN
0022-3263

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A number of primary and secondary amines have been rapidly methylated under microwave-enhanced conditions using formic acid-formaldehyde mixtures, providing a route to 2 H(D)-containing compounds and the potential for 3 H(T), 11 C, 13 C and 14 C labelling.