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Cyclisation of 1,2-dioxines containing tethered hydroxyl and carboxylic acid functionality: synthesis of tetrahydrofurans and dihydrofuran-2(3H)-ones

✍ Scribed by Ondrej Zvarec; Thomas D. Avery; Dennis K. Taylor; Edward R.T. Tiekink

Book ID: 108283189
Publisher: Elsevier Science
Year: 2010
Tongue: French
Weight: 358 KB
Volume: 66
Category: Article
ISSN: 0040-4020
DOI: 10.1016/j.tet.2009.11.068

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## Abstract 2‐^2^H, 2,3‐^2^H~2~ and 2,2‐^2^H~2~ ‐ short chain carboxylic acids were synthesized. Monodeuteration at the 2‐position of the carboxylic acids was achieved via decarboxylation of the corresponding carboxyldeuterated 2‐alkylmalonic acids. 2,3‐Dideuteration was achieved via catalytic deut