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Cyclic Phosphorochloridites and Phosphorochloridates Derived from Bromocalix[4]resorcinolarenes

✍ Scribed by A. N. Grigor'eva; E. A. Krasil'nikova; E. L. Gavrilova; A. R. Burilov; W. D. Habicher; M. A. Pudovik; A. I. Konovalov

Book ID: 111608345
Publisher: Springer
Year: 2003
Tongue: English
Weight: 40 KB
Volume: 73
Category: Article
ISSN: 1070-3632
DOI: 10.1023/b:rugc.0000015977.12119.cd

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## Abstract cis‐3,4‐Di‐tert‐butylthiolane‐3,4‐diol (**__1__**) was treated with an equimolar amount of thionyl chloride in the presence of triethylamine or pyridine in several solvents of different polarity to furnish two diastereomeric sulfites **__2a__** and **__2b__** generally in excellent comb