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(CuI)3P4S4: Preparation, Structural, and NMR Spectroscopic Characterization of a Copper(I) Halide Adduct with β-P4S4.

✍ Scribed by Sara Reiser; Gunther Brunklaus; Jung Hoon Hong; Jerry C.C. Chan; Hellmut Eckert; Arno Pfitzner

Publisher
John Wiley and Sons
Year
2010
Weight
37 KB
Volume
33
Category
Article
ISSN
0931-7597

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(CuI)(3)P(4)S(4) is obtained by reaction of stoichiometric amounts of CuI, P, and S in evacuated silica ampoules. The yellow compound consists of monomeric beta-P(4)S(4) cage molecules that are separated by hexagonal columns of CuI. (CuI)(3)P(4)S(4) crystallizes isotypic to (CuI)(3)P(4)Se(4) in the

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