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Cs3Nb2X9 (X = Cl, Br, J) und Rb3Nb2Br9

✍ Scribed by A. Broll; H.G. von Schnering; H. Schäfer

Book ID
116011591
Publisher
Elsevier Science
Year
1970
Weight
200 KB
Volume
22
Category
Article
ISSN
0022-5088

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Synthesis and Crystal Structures of Cs5Nb2S4X9 – Double Salts Containing New Cluster Anions [Nb2(μ-S2)2X8]4– (X = Cl, Br)
✍ Maxim Sokolov; Hideo Imoto; Taro Saito; Vladimir Fedorov 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 German ⚖ 197 KB 👁 2 views

Bis(disulfide) bridged Nb(+4) cluster halide complexes [Nb 2 S 4 X 8 ] 4± (X = Cl, Br) were prepared by acid hydrolysis of [Nb 2 S 4 (NCS) 8 ] 4± in concentrated aqueous HCl or HBr, solution from which they can be isolated as double salts Cs 5 [Nb 2 S 4 X 8 ]X (X = Cl, 1; X = Br, 2). The crystal st