Crystallization of chiral compounds 3. 3-phenoxypropane-1,2-diol and 3-(2-halophenoxy)propane-1,2-diols
✍ Scribed by D. V. Zakharychev; S. N. Lazarev; Z. A. Bredikhina; A. A. Bredikhin
- Publisher
- Springer
- Year
- 2006
- Tongue
- English
- Weight
- 390 KB
- Volume
- 55
- Category
- Article
- ISSN
- 1573-9171
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## Abstract A convenient procedure has been developed for the synthesis of ^14^C‐3‐chloropropan‐1, 2‐diol (α‐chlorohydrin, **I**) from ^14^C‐glycerol which can also be applied to the preparation of ^14^C‐3‐bromopropan‐1, 2‐diol (α‐bromohydrin, **III**). These two compounds can be converted, respect
Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.003 A Ê R factor = 0.051 wR factor = 0.123 Data-to-parameter ratio = 12.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.