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Crystal studies of musk compounds. V. Structure of 1-(1,2,6,7,8,8a-hexahydro-3,6,6,8a-tetramethylacenaphthylen-4-yl)ethan-1-one

✍ Scribed by De Ridder, D. J. A. ;Goubitz, K. ;Schenk, H.


Book ID
114510485
Publisher
International Union of Crystallography
Year
1994
Tongue
English
Weight
322 KB
Volume
50
Category
Article
ISSN
0108-2701

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## Abstract The 6‐(3‐hydroxypropylamino)‐3‐methylpyrimidine‐2,4‐dione (1) did not afford the expected 6‐(3‐chloro‐propylamino)‐ derivative on reaction with thionyl chloride, but, instead, the pyrimidine rings were joined __via__ a sulfur bridge to give 9,9′‐thiobis(1,2,3,4,7,8‐hexahydro‐7‐melnyl‐6_