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Structure of 3,4,5,6,7,8-hexahydro-1-methyl-1H-2-benzoxecine-3,8-dione

✍ Scribed by Batchelor, R. J. ;Einstein, F. W. B.


Book ID
114507960
Publisher
International Union of Crystallography
Year
1991
Tongue
English
Weight
241 KB
Volume
47
Category
Article
ISSN
0108-2701

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9,9′-Thiobis-(1,2,3,4,7,8-hexahydro-7-me
✍ Ondrej Šimo; Alfonz Rybár; Juraj Alföldi; Vladimír Pätoprstý 📂 Article 📅 1999 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 292 KB

## Abstract The 6‐(3‐hydroxypropylamino)‐3‐methylpyrimidine‐2,4‐dione (1) did not afford the expected 6‐(3‐chloro‐propylamino)‐ derivative on reaction with thionyl chloride, but, instead, the pyrimidine rings were joined __via__ a sulfur bridge to give 9,9′‐thiobis(1,2,3,4,7,8‐hexahydro‐7‐melnyl‐6_