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Crystal studies of musk compounds. I. 4-tert-Butyl-3-methoxy-2,6-dinitrotoluene (musk ambrette)

✍ Scribed by De Ridder, D. J. A. ;Goubitz, K. ;Schenk, H.

Book ID
114506719
Publisher
International Union of Crystallography
Year
1990
Tongue
English
Weight
320 KB
Volume
46
Category
Article
ISSN
0108-2701

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Synthesis of tritium labeled musk xylene
Synthesis of tritium labeled musk xylene, [3H] 5-tert-butyl-2,4,6-trinitro-m-xylene
✍ Masamichi Fukuoka; Seiichi Nambaru; Akira Tanaka πŸ“‚ Article πŸ“… 1991 πŸ› John Wiley and Sons 🌐 French βš– 296 KB

## Abstract Synthesis of ^3^H‐musk xylene (MX) was carried out by two schemes. Nitration of ^3^H‐5‐tert‐butyl‐__m__‐xylene (3) decreased in the ^3^H‐incorporation ratio. Reduction of MX‐bromide (6) with NaB^3^H~4~ gave the highly labeled MX (8) and another bromide (7) gave 9 with tritium atom produ