Crystal structures of an isomeric pair of 3-methylthio-5-amino-1,2,4-triazoles
✍ Scribed by A. Kálmán; L. Párkányi; J. Reiter
- Publisher
- Elsevier Science
- Year
- 1984
- Tongue
- English
- Weight
- 513 KB
- Volume
- 118
- Category
- Article
- ISSN
- 0022-2860
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The title compound (C 15 H 12 N 3 OSCl) crystallizes in the monoclinic space group P2 1 /n with a = 11.211( 3), b = 8.106(2), c = 17.494(4) Å, β = 104.49(2)º, V = 1539.2(7) Å 3 , Z = 4, D cal = 1.371 Mg/m 3 at T = 293 K. The structure was solved by direct methods and refined by full-matrix least-squ
## Abstract Isomeric type 1 and 2 amino‐1,2,4‐triazoles condensed with thiazole, thiazine and thiazepine rings were synthesised from 5‐amino‐2,3‐dihydro‐1__H__‐1,2,4‐triazol‐3‐thione and α,ω‐dihaloalkanes through the 5‐amino‐3‐(ω‐haloalkylthio)‐1__H__‐1,2,4‐triazole intermediates. The reaction cond
## Abstract For Abstract see ChemInform Abstract in Full Text.