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Crystal structures of (±)-1,4-di-O-benzoyl-2,3-O-isopropylidene-myo-inositol and (±)-1,4-di-O-benzoyl-5,6-O-isopropylidene-myo-inositol: a conformational analysis

✍ Scribed by Sung-Kee Chung; Young-Tae Chang; Dongmok Whang; Kimoon Kim

Book ID
108309657
Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
377 KB
Volume
295
Category
Article
ISSN
0008-6215

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An efficient method for the resolution of 1,2:4,5-di-O-isopropylidene-myo-inositol has been developed. The diketal was converted to diastereomeric 3,6-di-O-mandelates by the reaction with (S)-O-acetylmandeloyl chloride. Both the diastereomers could be separated by sequential crystallization in multi