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Crystal structures, electronic properties and structural pathways of four [Cu(phen)2Cl][Y] complexes (phen = 1,10-phenanthroline; Y = BF4−·0.5H2 O, PF6−, CF3SO3−·H2O or BPh4−)

✍ Scribed by Murphy, Gillian; Nagle, Pat; Murphy, Brian; Hathaway, Brian

Book ID
119971322
Publisher
The Royal Society of Chemistry
Year
1997
Tongue
English
Weight
135 KB
Volume
15
Category
Article
ISSN
1472-7773

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Blue crystals of Cu 2 (phen) 2 (H 2 O) 2 (C 5 H 6 O 4 ) 2 were obtained from a CH 3 OH±H 2 O solution containing CuCl 2 , 1,10-phenanthroline (phen), glutaric acid and Na 2 CO 3 . The crystal structure (monoclinic, P2 1 /c (no. 14), a = 10.271(1), b = 10.595(1), c = 15.585(1) A Ê , b = 107.105(3)°,

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The crystal and molecular structures of [Mn(phen)-(OHz)C13] (1) and [Mn(acac)2(OHE)/]C104"2H20 (2) were determined. A comparison is made of the Jahn-Teller distortion in these compounds with those observed in other manganese(III) complexes with monodentate axial ligands.