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Crystal Structure of the Antibiotic Monensin Similarities and Differences between Free Acid and Metal Complex

✍ Scribed by W. K. Lutz; F. K. Winkler; J. D. Dunitz

Publisher: John Wiley and Sons
Year: 1971
Tongue: German
Weight: 368 KB
Volume: 54
Category: Article
ISSN: 0018-019X
DOI: 10.1002/hlca.19710540419

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✦ Synopsis

41 (70), 27 (40). -Das dancbcn zu -45% cntstandcnc cis-P-Hymentheren (4) zeigte [ a ] g = + 161". 9. (R)-( -)-trans-Z,6-Dimethyloctatrien-1, 4,7 (9; trans-Achillene). 3,2 g trans-Alkohol 7 ([a]? = -5.9") wurden wie vorstehend beschrieben mit 0,8 g B(OH), bei 130"/150 Torr dehydratisiert. . !. us den1 nach Uestillation erhaltenen Gemisch der Triene 9 und 3 (Bildungsverhaltnis -1 : 1) isolicrtcn wir 1,1 g rcines 9 durch praparat. Gas-Chromatographie unter den eingangs erwahnten Redingungcn: Rt = 3,6 Min.; [a]: = -3,8"; ttg = 1,4461; d y = 0,

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