Bei der Kondensation von 4‐Chlorphenyl‐propiolsäuremethylester mit 2‐Anilino‐2‐imidazol entsteht die Titelverbindung, deren Struktur durch eine Röntgenstrukturanalyse bewiesen wurde. Die Kristalle gehören in die azentrische, orthorhombische Raumgruppe Pna2~1~, __a__ = 13,49, __b__ = 10,52 und __c__
Crystal structure of 4,5-bis-phenyl-8a-phenyl-3,4,4a,5,6,8a-hexahydro-1H,8H-pyrimido[4.5-d]pyrimidine-2,7-dione
✍ Scribed by M. M. Kurbanova; A. V. Kurbanov; A. B. Novruzova; V. N. Khrustalev; A. M. Magerramov
- Publisher
- SP MAIK Nauka/Interperiodica
- Year
- 2010
- Tongue
- English
- Weight
- 146 KB
- Volume
- 51
- Category
- Article
- ISSN
- 0022-4766
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The title compound, C 14 H 18 N 2 O 2 S, which was obtained from an extended Biginelli reaction, contains a pyran ring with a chair conformation, a pyrimidine ring with a half-chair conformation and a benzene ring. The crystal structure is stabilized by an intermolecular hydrogen-bond network.