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Crystal and molecular structure of the depsipeptide ionophore Hexadecaisoleucinomycin, cyclo-[-(D-Ile-L-Lac-L-Ile-D-Hyi)4-] (C80H136N8O24)

✍ Scribed by V. Z. Pletnev; V. T. Ivanov; D. A. Langs; P. Strong; W. L Duax

Publisher: Wiley (John Wiley & Sons)
Year: 1992
Tongue: English
Weight: 644 KB
Volume: 32
Category: Article
ISSN: 0006-3525
DOI: 10.1002/bip.360320710

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The crystal and molecular structure of the valinomycin analogue, cyclo [(D-Val-L-Lac-L-Ala-D-Hyi) 2 (D-Val-L-Lac-L-Val-D-Hyi)] has been solved by x-ray direct methods using the ''Shake and Bake'' procedure. The crystals, grown from a mixture of octane/CH 2 Cl 2 , belong to space group P2 1 (Z Å 4) w

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Hyi-0-Val-t-Hyi) . 2H20 has been solved by x-ray direct methods. The crystals (grown from a mixture of octane/CH2C12) are an orthorhombic, centrosymmetric space group Pbca, cell parameters a = 11.458( 2), b = 25.613(3), c = 23.691 (3) k, Z = 4; therefore the molecule lies on a center of inversion i