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Cross-Coupling Reactions of Organosilicon Compounds in the Stereocontrolled Synthesis of Retinoids

✍ Scribed by Julián Bergueiro; Dr. Javier Montenegro; Fermín Cambeiro; Prof. Dr. Carlos Saá; Prof. Dr. Susana López

Book ID
112019934
Publisher
John Wiley and Sons
Year
2012
Tongue
English
Weight
546 KB
Volume
18
Category
Article
ISSN
0947-6539

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Stereocontrolled synthesis of retinoids
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✍ Rosana Alvarez; Beatriz Iglesias; Angel R. de Lera 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 923 KB

The retinal analogues ( 13Z)-13-bromo-13-desmethylretinal (3) and ( 13E)-20,20,20-trifluororetinal (4) have been efficiently synthesized using the palladium-catalyzed cross-coupling of boronic acid 8 and electrophiles 9 and 10, respectively. For the first analogue, the coupling of 8 and the gem-dibr