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Coupling of chromatography and NMR. 3—study of flowing gas chromatographic fractions by proton magnetic resonance

✍ Scribed by Joachim Buddrus; Helmut Herzog


Publisher
John Wiley and Sons
Year
1981
Tongue
English
Weight
245 KB
Volume
15
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

A procedure is described which allows the recording of ^1^H NMR spectra from gas chromatographic (GC) fractions flowing through the magnetic field with a velocity of c. 0.6 cm/s. The spectra are obtained by the pulse Fourier transform technique; the beginning and the termination of the pulse sequence is timed according to the chromatogram from a thermal conductivity detector. The line width of the signals in the NMR spectra is 2 Hz.


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