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Coupling of Allenes with μ-Alkylidyne Ligands in Diiron Complexes: Synthesis of Novel Bridging Thio- and Aminobutadienylidene Complexes

✍ Scribed by Luigi Busetto; Fabio Marchetti; Mauro Salmi; Stefano Zacchini; Valerio Zanotti

Publisher: John Wiley and Sons
Year: 2008
Tongue: English
Weight: 334 KB
Volume: 2008
Category: Article
ISSN: 1434-1948
DOI: 10.1002/ejic.200800048

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## Abstract A new μ‐oxodiiron(III) complex [{Fe^III^(bpc)(H~2~O)}~2~O] (1) with the bis(picolinamide) N~4~ in‐plane ligand 4,5‐dichloro‐1,2‐bis(pyridine‐2‐carboxamido)benzene (H~2~bpc) has been prepared by the reaction of [Fe(bpc)Cl(H~2~O)] with a stoichiometric amount of cyanide, and characterized