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Correlation of carbon-13 and nitrogen-15 chemical shifts in selectively and uniformly labeled proteins by heteronuclear two-dimensional NMR spectroscopy

✍ Scribed by Westler, William M.; Stockman, Brian J.; Hosoya, Yoshiko.; Miyake, Yoko.; Kainosho, Masatsune.; Markley, John L.

Book ID: 127211298
Publisher: American Chemical Society
Year: 1988
Tongue: English
Weight: 967 KB
Volume: 110
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja00226a057

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## Abstract The complete assignment of the proton and carbon chemical shifts of 6‐__O__‐acetyl‐2,3,4‐tri‐__O__‐(3__S__‐methylpentanoyl)‐α‐D‐glucopyranosyl‐β‐D‐fructofuranoside, a naturally occurring flavor precursor of tobacco, is presented. These assignments were made by comparison of the spectra