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Assignment of proton and carbon-13 spectra of a sucrose ester from tobacco by inverse detected two-dimensional heteronuclear correlated NMR spectroscopy

✍ Scribed by David S. Himmelsbach; Herman van Halbeek; Richard F. Arrendale; Ray F. Severson

Publisher
John Wiley and Sons
Year
1990
Tongue
English
Weight
519 KB
Volume
28
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

The complete assignment of the proton and carbon chemical shifts of 6‐O‐acetyl‐2,3,4‐tri‐O‐(3__S__‐methylpentanoyl)‐α‐D‐glucopyranosyl‐β‐D‐fructofuranoside, a naturally occurring flavor precursor of tobacco, is presented. These assignments were made by comparison of the spectra obtained from ^1^H‐detected heteronuclear multiple quantum coherence and ^1^H‐detected heteronuclear multiple‐bond connectivity two‐dimensional NMR experiments.

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