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Copper(I) Isocyanide and Phosphane Complexes of Fluorinated Mono- and Bis(pyrazolyl)borates

✍ Scribed by H. V. Rasika Dias; Giancarlo Gioia Lobbia; Grazia Papini; Maura Pellei; Carlo Santini

Publisher
John Wiley and Sons
Year
2009
Tongue
English
Weight
461 KB
Volume
2009
Category
Article
ISSN
1434-1948

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## Abstract TMEDA‐free (TMEDA: tetramethylethylenediamine) LiCH~2~SMe is a suitable reagent for the selective introduction of (methylthio)methyl groups into PhBBr~2~ and its __p__‐silylated derivative Me~3~Siο£ΏC~6~H~4~ο£ΏBBr~2~. The resulting compounds, R\*ο£ΏC~6~H~4~ο£ΏB(Br)(CH~2~SMe) (R\*=H: 2; R\*=SiMe