Copper-Mediated Simple and Efficient Synthesis of Tribenzohexadehydro[12]annulene and Its Derivatives.
β Scribed by Masahiko Iyoda; Siriwan Sirinintasak; Yoshihiro Nishiyama; Anusorn Vorasingha; Fatema Sultana; Kazumi Nakao; Yoshiyuki Kuwatani; Haruo Matsuyama; Masato Yoshida; Yoshihiro Miyake
- Publisher
- John Wiley and Sons
- Year
- 2004
- Weight
- 23 KB
- Volume
- 35
- Category
- Article
- ISSN
- 0931-7597
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π SIMILAR VOLUMES
1 -Methyl-5-aminopyrazole can be tosylated t o give ( 4 ) , R = CH3, m.p. 188-190Β°C, the structure of which has been substantiated by the characteristic position of its sulfonyl absorption [5] in the infrared and by the synthesis [4] of
## Abstract magnified image Reaction of 4βphenylthiosemicarbazide with dialkyl acetylenedicarboxylate in CH~2~Cl~2~ at 0Β°C lead to construction of alkyl 3βaminoβ2βphenyliminothiazolidineβ4βoneβ5βylidene acetate in a few minutes and good yields. Alternatively, the use of thiosemicarbazide has given