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Copper-Catalyzed Synthesis of N-Sulfonyl-1,2,3-triazoles: Controlling Selectivity.

✍ Scribed by Eun Jeong Yoo; Maarten Ahlquist; Seok Hwan Kim; Imhyuck Bae; Valery V. Fokin; K. Barry Sharpless; Sukbok Chang

Publisher
John Wiley and Sons
Year
2007
Weight
25 KB
Volume
38
Category
Article
ISSN
0931-7597

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Copper-Catalyzed Synthesis of N-Unsubsti
Copper-Catalyzed Synthesis of N-Unsubstituted 1,2,3-Triazoles from Nonactivated Terminal Alkynes
✍ Tienan Jin; Shin Kamijo; Yoshinori Yamamoto πŸ“‚ Article πŸ“… 2004 πŸ› John Wiley and Sons 🌐 English βš– 86 KB

## Abstract The [3+2] cycloaddition of nonactivated terminal alkynes and trimethylsilyl azide proceeded smoothly in the presence of Cu^I^ catalyst and DMF/MeOH, to give the corresponding __N__‐unsubstituted triazoles in good to high yields. The reaction most probably proceeds through the in situ fo