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Coordination Chemistry of a Novel Tetramacrocyclic Ligand Derived from 1,4,7-Triazacyclononane: Synthesis, Structure, and Properties of Nickel(II) and Copper(II) Complexes

✍ Scribed by Graham, Bim; Grannas, Martin J.; Hearn, Milton T. W.; Kepert, Christopher M.; Spiccia, Leone; Skelton, Brian W.; White, Allan H.

Book ID: 126033983
Publisher: American Chemical Society
Year: 2000
Tongue: English
Weight: 194 KB
Volume: 39
Category: Article
ISSN: 0020-1669
DOI: 10.1021/ic991082z

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## Abstract The synthesis, X‐ray crystal structure and magnetic properties of two oxalato‐bridged dinuclear Cu^II^ complexes, [L‐Cu(μ‐ox)Cu‐L](ClO~4~)~2~, where ox = oxalate and L = 1,4,7‐trimethyl‐1,4,7‐triazacyclononane (Me~3~tacn) or 1‐benzyl‐4,7‐dimethyl‐1,4,7‐triazacyclononane (BzMe~2~tacn) ar