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Conversion of [14C]pentachloronitrobenzene in onions

✍ Scribed by S. Begum; I. Scheunert; A. Haque; W. Klein; F. Korte

Book ID
119026960
Publisher
Elsevier Science
Year
1979
Tongue
English
Weight
734 KB
Volume
11
Category
Article
ISSN
0048-3575

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Synthesis of pentachloronitrobenzene-14C
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## Abstract Pentachloronitrobenzene‐^14^C~6~ was synthesized in 81.7% yield by exhaustive chlorination of nitrobenzene‐^14^C~6~. Hexachlorobenzene‐^14^C~6~ was produced in 11% yield as a byproduct of the reaction.

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## Abstract Starting with benzene‐U‐^14^C pentachloronitrobenzene‐U‐^14^C has been prepared by nitration followed by chlorination with antimony pentachloride in the presence of aluminum chloride.