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Convergent Approach to Pumiliotoxin Alkaloids. Asymmetric Total Synthesis of (+)-Pumiliotoxins A, B, and 225F

✍ Scribed by Aoyagi, Sakae; Hirashima, Shintaro; Saito, Kosuke; Kibayashi, Chihiro

Book ID
125543346
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
170 KB
Volume
67
Category
Article
ISSN
0022-3263

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## Abstract This article describes in detail the first total synthesis of grandisine alkaloids, grandisinesβ€…B, D, and F, which show affinity for the human δ‐opioid receptor. The key steps in this synthesis are construction of the isoquinuclidinone moiety of **2** by intramolecular imine formation a