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Convenient Synthesis of Thiol Esters from Acyl Chlorides and Disulfides Using Zn/AlCl3

✍ Scribed by Moslem M. Lakouraj; Barahman Movassagh; Zahra Fadaei

Book ID
106215099
Publisher
Springer Vienna
Year
2002
Tongue
English
Weight
42 KB
Volume
133
Category
Article
ISSN
0026-9247

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✍ Barahman Movassagh; Mozhgan Navidi πŸ“‚ Article πŸ“… 2008 πŸ› Elsevier Science 🌐 French βš– 161 KB

A simple, general, and highly regioselective procedure has been developed for the one-pot synthesis of b-hydroxysulfides in good yields from various styrenes and disulfides by cleavage of the S-S bond with a Zn/AlCl 3 system in aqueous acetonitrile at 80 Β°C and in the presence of oxygen.